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抗生素废水的GC-MS分析与显色物质的初步确定
引用本文:赵立军,郭磊,陈进富,郭春梅,靳炜.抗生素废水的GC-MS分析与显色物质的初步确定[J].环境工程学报,2009,3(10):1830-1834.
作者姓名:赵立军  郭磊  陈进富  郭春梅  靳炜
作者单位:1. 中国石油大学(北京)环境中心,北京,102249
2. 中国石油大学(北京)环境中心,北京,102249;中国石油大学(北京)化学科学与工程学院,北京,102249
3. 中国科学院生态环境研究中心,北京,100085
摘    要:为确定抗生素废水中有机污染物构成和显色物质,以二氯甲烷为萃取剂,萃取废水中的有机物,经过浓缩纯化后,利用气相色谱质谱联用(GC-MS)技术对制药废水中的有机成分进行了分析鉴定,结合计算机质谱图库,定性确定了废水中60种有机污染物。其中,脂类为主要污染物成分,经对脱色后的废水进一步GC-MS分析后,初步确定油酸甲酯为此类抗生素废水的主要显色有机物。

关 键 词:抗生素废水  GC-MS  显色物质

GC-MS analysis of antibiotic wastewater and preliminary determination of color materials
Zhao Lijun,Guo Lei,Chen Jinfu,Guo Chunmei and Jin Wei.GC-MS analysis of antibiotic wastewater and preliminary determination of color materials[J].Techniques and Equipment for Environmental Pollution Control,2009,3(10):1830-1834.
Authors:Zhao Lijun  Guo Lei  Chen Jinfu  Guo Chunmei and Jin Wei
Institution:1.Environment Center,China University of Petroleum(Beijing),Beijing 102249,China,1.Environment Center,China University of Petroleum(Beijing),Beijing 102249,China;2.School of Chemical and Engineering, China University of Petroleum(Beijing),Beijing 102249,China;,1.Environment Center,China University of Petroleum(Beijing),Beijing 102249,China,1.Environment Center,China University of Petroleum(Beijing),Beijing 102249,China and 3.Research Center for Eco-Environment Sciences,Chinese Academy of Sciences,Beijing 100085,China
Abstract:To determine the composition of organic pollutants and the color materials in the antibiotics wastewater, using dichloromethane to extract the organic matter in waste water. After concentration and purification, the gas chromatography mass spectrometry (GC-MS) technology was used to analyze and identify the organic component in the pharmaceutical waste water. Combined with mass spectrometry library computer,it is identified that there are 60 kinds of organic pollutants in wastewater .And the lipid components are the main pollutants. After further analysis of the depolarization wastewater, it is determined that the initial oil methyl ester is the main color organic matter in the antibiotics wastewater.
Keywords:antibiotic wastewater  GC-MS  color material
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