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鱼组织中多环芳烃的测定
引用本文:储少岗,徐晓白.鱼组织中多环芳烃的测定[J].环境科学学报,1994,14(2):229-235.
作者姓名:储少岗  徐晓白
作者单位:中国科学院生态环境研究中心
摘    要:研究了鱼体中2-5环多环芳烃的分析方法,方法包括皂化,萃取,氧化铝柱色谱分组、SephadexLH-20凝胶色谱净化,以及气相色谱和高效液相色谱方法分离测定,其方法对多环芳烃的添加回收率在60%之间,检测限为0.1ppb。应用本方法测定了北京地区两个鱼样体内多环芳烃的含量。

关 键 词:多环芳烃    气相色谱  液相色谱
收稿时间:1992/8/29 0:00:00

ANALYSIS OF POLYCYCLIC AROMATIC HYDROCARBONS IN FISH TISSUE
Chu Shaogang and Xu Xiaobai.ANALYSIS OF POLYCYCLIC AROMATIC HYDROCARBONS IN FISH TISSUE[J].Acta Scientiae Circumstantiae,1994,14(2):229-235.
Authors:Chu Shaogang and Xu Xiaobai
Institution:Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing 100085 and Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing 100085
Abstract:A method is described for the determination of polycyclic aromatic hy-drocarbons(PAHs with 2-5 rings in fish tissue. The analytical procedure includes following steps:saponification,extraction,column chromato-graphy on alumina,clean-up with gel permeation chromatography,gas chromatography and high performance liquid chromatography with UV and fluorescence detectors.The recoveries ranged from 60% to 98% for PAHs and the detection limit is 0.1 ppb.Results of fish samples are presen-ted. One of the samples comes from a reservoir and the other comes from afishing ground.
Keywords:PAHs  fish  GC  HPLC
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