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COD快速测定法
引用本文:陈立波,李凤亭. COD快速测定法[J]. 化工环保, 2004, 24(6): 455-457
作者姓名:陈立波  李凤亭
作者单位:同济大学,环境科学与工程学院,上海,200092;吉林化工学院,环境科学与工程系,吉林,吉林,132022;同济大学,环境科学与工程学院,上海,200092
摘    要:以用时30min的半微量密闭微波消解法取代COD国标测定中的重铬酸钾回流法,改进后的方法精密度小于5.15%,准确度达到102%,COD测定下限为51mg/L。该法节省时间、取样量少、成本低,适用于大批量水样的快速测定。

关 键 词:化学需氧量  微波消解  快速测定
文章编号:1006-1878(2004)06-0455-03
修稿时间:2004-02-02

Rapid Determination of Chemical Oxygen Demand
Chen Libo,Li Fengting. Rapid Determination of Chemical Oxygen Demand[J]. Environmental Protection of Chemical Industry, 2004, 24(6): 455-457
Authors:Chen Libo  Li Fengting
Abstract:A method for rapid determination(in 30 min)of COD by microwave counteracting in closed condition and with semi - trace quantity was developed, which could substitute the national standard method with bichrome. The precision of the method is less than 5.15% , the accuracy is 102% ,and the detection limit is 51 mg/L. It has the advantages of rapidity,using less sample and low cost. It is appropriate to the determination of water sample in great batches.
Keywords:chemical oxygen demand  microwave counteracting  rapid determination
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