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41.
实验室仪器设备的准确性是检测结果准确性的重要保证,按规定和要求对仪器进行期间核查,可以确保检测数据的准确可靠。结合仪器设备期间核查的实例说明期间核查是维持设备校准状态的可信度的重要手段。 相似文献
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Determination of alkali-labile phosphoprotein phosphorus from fish plasma using the Tb^3+-tiron complex as a fluorescence probe 总被引:1,自引:0,他引:1
A sensitive method based on the fluorescence quenching effect of the Tb^3+-Tiron complex is proposed for the determination of alkali-labile phosphoprotein phosphorus (ALP) released from fish plasma. The detection limit was 5.4 ng/ml (S/N=2), and the relative standard deviation of the quenching effect (6 replicates) was 4.6%. The results obtained by the proposed method were in good agreement with those obtained by the colorimetric assay. The advantages of the present method are its relatively simple detection procedure, the lack of toxic organic solvents, and high sensitivity. 相似文献
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水中总氮测定相关问题的实验探讨 总被引:1,自引:0,他引:1
通过对国家标准测定方法《碱性过硫酸钾消解紫外分光光度法》进行水样中总氮的测定,进一步理解在220nm、275nm波长处进行吸光度测定的重要性。并提出:在已经知道水样中没有氨氮、亚硝酸盐氮,只有硝酸盐氮的情况下.就能通过快速的方法一即不加氧化剂、不加压,可以进行总无机氮的测定。快速测定无机总氮对于工程应用来说很有意义。因为国标的方法需要半天时间测定。而用此方法则仅需几分钟就可完成测定。、另外对于有机物对于测定结果的影响,参考吸光度比值(A275/A220×100%)应小于20%,越小越好,超过时应予鉴别。 相似文献
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Xiaojiao Chen Minjian Chen Bo Xu Rong Tang Xiumei Han Yufeng Qin Bin Xu Bo Hang Zhilei Mao Weiwei Huo Yankai Xia Zhengfeng Xu Xinru Wang 《Chemosphere》2013
Widespread use of phenols has led to ubiquitous exposure to phenols. In experimental animals, phenols increased resorptions, reduced live litter size and fetal body weights. However, there are limited epidemiological evidences of the relationships between exposure to phenols and pregnancy outcomes. We evaluated the associations between parental urinary levels of various phenols and spontaneous abortion in a Chinese population residing in the middle and lower reaches of the Yangtze River. A case-control study was conducted that included 70 case couples with medically unexplained spontaneous abortion and 180 control couples who did not have a history of spontaneous abortion and had at least one living child. Both parental urinary phenols were measured by ultra-high performance liquid chromatography-tandem mass spectrometry including bisphenol A (BPA), benzophenone-3 (BP-3), 2,3,4-trichlorophenol (2,3,4-TCP), pentachlorophenol (PCP), 4-n-octylphenol (4-n-OP) and 4-n-nonylphenol (4-n-NP). Compared with the low exposure group, there was an increased risk of spontaneous abortion with high paternal urinary PCP concentration [odds ratio (OR) = 2.09, 95% Confidence Interval (CI), 1.05–4.14], and maternal exposure to 4-n-OP and alkylphenol(s) also significantly increased the risk of spontaneous abortion (OR = 2.21, 95% CI, 1.02–4.80; OR = 2.81, 95% CI, 1.39–5.65, respectively). Our study firstly provides the evidence that paternal PCP exposure, maternal 4-n-OP and alkylphenol(s) exposure are associated with spontaneous abortion in humans. 相似文献
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Jorge Rickards 《Journal of environmental radioactivity》2010,101(5):333-337
The functioning of radon diffusion chambers was studied using the Monte Carlo code RAMMX developed here. The alpha particles from radon are assumed randomly produced in the volume of the cylinder, and those from the progeny are assumed to originate randomly at the cylindrical surface. The energy spectrum, the distribution of incident angles, and the distribution of path lengths of the alpha particles on the detector were obtained. These quantities vary depending on input parameters such as initial alpha particle energy, radius and depth of the diffusion chamber, detector size and atmospheric pressure. The calculated energy spectrum for both 222Rn and 220Rn was compared with experiment, permitting the identification of each peak and its origin, and a better understanding of radon monitoring. Three aspects not considered in previous calculations are progeny alphas coming from surfaces of the monitor, taking into account the atmospheric pressure, and including the isotope 220Rn. 相似文献