利用薄片穿透法确定铝合金最大蚀坑深度

目的研究铝合金最大蚀坑深度与环境试验时间的对应关系,为新型合金服役前的耐蚀性评级和结构件服役过程中的剩余寿命预测提供技术基础。方法利用光学显微镜、扫描电镜分析海洋大气环境中新型铝合金的腐蚀类型,并利用薄片穿透法研究铝合金薄片最大蚀坑深度与试验时间的对应关系。结果经过海洋大气环境暴露试验后,2A97铝合金发生了深入合金内部的严重点蚀,检测薄片试样背面电解液的出现时间,可以确定环境试验中蚀坑穿透薄片试样的时间。通过测量不同厚度薄片试样的穿透时间,可以确定最快生长局部腐蚀点的深度和时间的关系。结论中性盐雾试验环境下,达到相同的最大蚀坑深度,2A97铝合金与AA2024铝合金用时基本相当。     

我国东部沿海地区差距状况以及经济低谷地区的崛起

我国是区域发展差异巨大的大国之一，存在着多种尺度的区域发展差异。从中小尺工区域差异的角度，分析了我国东部沿海地区内部发展差距扩大趋势有其影响，可以看出，东部沿海地区在经济快速发展的同时，也存在着经济相对落后的低谷地区。沿海经济低谷地区分布相对集中于香港－－珠江三角洲、上海－长江三角洲、京津唐－环渤海三个经济隆起带之间，处于省际交界处。按照类型可以分为黄泛平原区、丘陵山区和沿海库区。东部经济低谷地区区位条件相对比较落后，交通可达性较差，产业结构单一，城市化水平发展严重滞后，社会经济发展比较缓慢，这些不利因素制约着该地区经济和社会的发展。根据崛起机制和途径，低谷地区发展呵以分为资源转换型、非国有经济推动型和外资推动型。建议国家修筑贯穿沿海经济低谷地区的东部沿海铁路大通道，降低沿海经济低谷地区设定标准，加快农业产业化发展，对特殊贫困地区实行特殊优惠政策，从而促进东部沿海地区经济协调发展。     

Experimental study on non-destructive testing of rock bolts based on pseudo-random signal

The quality of rock bolt anchoring is closely related to the stability and safety of underground engineering and slope protection. In this paper, non-destructive testing of rock bolts is proposed based on pseudo-random signal, owing to the deficiencies of the conventional detecting method of stress wave reflection. The characteristics of pseudo-random signal for non-destructive testing of rock bolts are introduced. And the rock bolts are tested in the experiment, the time of reflection wave is identified and the length of rock bolts is calculated through cross correlation analysis between the extracted wavelet signal and the test signal. It is proved that the testing results of non-destructive testing methods based on pseudo-random signal are of low deviation. The experiment has shown that non-destructive testing of rock bolts based on pseudo-random signal is feasible with high precision.     

埕岛油田海底管道漏磁检测与安全评估

提出了埕岛油田海底管道内缺陷漏磁检测需解决的主要问题,研发了325 mm管道内缺陷漏磁检测装置,确定了海底管道漏磁检测工艺流程,配套了管道检测发射装置、接受装置等相关设施,实现了海底管道的漏磁检测、缺陷分析和安全评估。     

高含硫气田试气与地面工程建设交叉作业安全管理方法初探

普光气田作为高含硫气田在国内大规模开发,尚属首例,在气田开发过程中没有可借鉴的经验.高含硫气井试气作业中易发生井喷、硫化氢泄漏等事故.普光气田地面工程建设施工难度大、地形复杂,按照工程进度要求,试气作业和地面集输工程施工两项作业交叉时必须实现“安全作业、安全施工”,这是普光气田开发的基本目标.通过制订安全管理制度、明确责任主体、服从业主统一管理等有效的安全管理方法,保证了目标的实现,获得安全管理经验,对今后高含硫气田大规模开发具有指导意义.     

加强危险场所电气安全检测,提高化工企业本质安全水平

针对近年来化工企业电气安全、防静电等事故多发的现状,本文通过对化工企业电气安全、防静电等安全设施存在的问题进行分析,阐述了化工企业电气安全、防静电设施存在的主要缺陷,强调了利用技术支撑手段对在用安全设施进行检测检验对提高企业本质安全水平的重要性,并对如何做好电气安全、防静电等安全设施的检测工作提出了建议。     

Pressurized liquid extraction of six tetracyclines from agricultural soils

Veterinary antibiotics used in agriculture can be introduced into the environment through land application of animal manure, accumulating in soils and groundwaters and posing a significant risk to human health and animal well-being. As the analysis of tetracyclines in soil is challenging due to their strong interaction with soil minerals and organic carbon, the objective of this study was to develop a reliable and reproducible method for quantitative analysis of chlortetracycline and oxytetracycline, and their respective metabolites in soils. A method based on pressurized liquid extraction (PLE) with in-cell clean-up was developed for the extraction of chlortetracycline and oxytetracycline and four likely metabolites from a set of four soils. Optimized conditions included a cell size of 22?mL, soil loading of 5?g, pH of 8.0, methanol:water ratio of 3:1, 50?°C, and two cycles. Soil extracts were analysed by high-performance liquid chromatography (HPLC) coupled with ion trap mass spectrometry (MS). Recoveries of seven tetracyclines from soil ranged from 41% to 110%. The limits of detection for tetracyclines were 0.08–0.3 µg g^?1 soil, and intra- and inter-day variation ranged from 0.12–0.34%. The proposed PLE method is suitable for quantification of tetracyclines in agricultural soils at typical concentrations expected in contaminated environments.     

锂电池检测的安全标准及安全防护研究

为评估并提高锂电池在使用、储存和运输过程中的安全,本文归纳总结了国内外锂电池安全检测的相关标准,对标准中测试项目异同作了重点分析和对比,并讨论了锂电池的安全风险及风险分级情况。同时,鉴于锂电池检测过程中可能出现的起火、爆炸等危险,探讨了电池检测过程的安全防护技术,并从样品区和试验区两方面提出了安全防护要求和建议。     

Effects of falling weight impact on industrial safety helmets used in conjunction with eye and face protection devices

Industrial workplaces pose concurrent hazards to the upper part of the head and the eyes. Under the circumstances, workers may use protective helmets in conjunction with protective goggles or spectacles. In order to assess the compatibility of this equipment, a method and a test stand for evaluating the behavior of safety helmets and protective goggles/spectacles upon the impact of a falling weight were designed. The results of tests concerning the displacement and deformation of helmets and spectacles/goggles, the forces acting on the helmets, as well as the forces exerted by the spectacles/goggles on the headform upon falling weight impact are presented. The results revealed the ways in which the tested equipment interacted with each other. The influence of equipment construction on the test results was analyzed and inferences concerning the safety of the studied protective devices were made. Some general construction guidelines were formulated for the compatibility of the equipment.     

Performance-based earthquake evaluation of a full-scale petrochemical piping system

Assessment of seismic vulnerability of industrial petrochemical and oil & gas piping systems can be performed, beyond analytical tools, through experimental testing as well. Along this line, this paper describes an experimental test campaign carried out on a full-scale piping system in order to assess its seismic behaviour. In particular, a typical industrial piping system, containing several critical components, such as elbows, a bolted flange joint and a Tee joint, was tested under different levels of realistic earthquake loading. They corresponded to serviceability and ultimate limit states for support structures as suggested by modern performance-based earthquake engineering standards. The so called hybrid simulation techniques namely, pseudo-dynamic and real time testing with dynamic substructuring, were adopted to perform seismic tests. Experimental results displayed a favourable performance of the piping system and its components; they remained below their yielding, allowable stress and allowable strain limits without any leakage even at the Near Collapse Limit State condition for the support structure. Moreover, the favourable comparison between experimental and numerical results, proved the validity of the proposed hybrid techniques alternative to shaking table tests.