Biodiesel production from vegetable oil and waste animal fats in a pilot plant

In this study, corn oil as vegetable oil, chicken fat and fleshing oil as animal fats were used to produce methyl ester in a biodiesel pilot plant. The FFA level of the corn oil was below 1% while those of animal fats were too high to produce biodiesel via base catalyst. Therefore, it was needed to perform pretreatment reaction for the animal fats. For this aim, sulfuric acid was used as catalyst and methanol was used as alcohol in the pretreatment reactions. After reducing the FFA level of the animal fats to less than 1%, the transesterification reaction was completed with alkaline catalyst. Due to low FFA content of corn oil, it was directly subjected to transesterification. Potassium hydroxide was used as catalyst and methanol was used as alcohol for transesterification reactions. The fuel properties of methyl esters produced in the biodiesel pilot plant were characterized and compared to EN 14214 and ASTM D6751 biodiesel standards. According to the results, ester yield values of animal fat methyl esters were slightly lower than that of the corn oil methyl ester (COME). The production cost of COME was higher than those of animal fat methyl esters due to being high cost biodiesel feedstock. The fuel properties of produced methyl esters were close to each other. Especially, the sulfur content and cold flow properties of the COME were lower than those of animal fat methyl esters. The measured fuel properties of all produced methyl esters met ASTM D6751 (S500) biodiesel fuel standards.     

XZKP型高效空塔喷淋烟气脱硫装置技术特点

介绍了XZKP型高效空塔喷淋烟气脱硫装置的技术原理、技术特点、中试及工业化试验的情况。该技术通过改进工艺和结构，在提高脱硫效率和脱硫剂循环利用率两项技术上成效显著，用户可在不增加装置投资的前提下，获得更高的效率和更低的运行成本。     

诱导喷嘴改进滤筒脉冲清灰效果的实验研究

改善清灰效果是提高滤筒除尘效率的关键和难点问题。运用自制脉冲喷吹实验台,采用诱导喷嘴(超音速引流喷嘴和气流散射器)对325 mm×660 mm滤筒进行脉冲喷吹清灰实验研究,并与采用普通喷吹孔的实验结果进行比较分析,得出采用诱导喷嘴时侧壁正压力峰值平均值是普通喷吹孔的1.465倍;且采用诱导喷嘴时各测点的不均衡系数为0.768～1.336,普通喷口为0.270～2.251,而不均衡系数越接近于1,其清灰效果越好;同时,采用诱导喷嘴时各测点基本在同一时刻达到正峰值。实验充分表明采用诱导喷嘴确保了滤筒长度方向上内壁清灰压力的均匀性,且对滤筒清灰效果有明显的改善作用。     

固定式可燃气体检测报警器运行管理中存在的问题及对策

针对固定式可燃气体检测报警器运行管理中存在的问题进行了分析,并提出整治措施.     

加速溶剂萃取-在线净化-液相色谱串联质谱法检测污泥堆肥样品中三氯生和三氯卡班

污泥堆肥样品基质复杂,其中三氯生（TCS）和三氯卡班（TCC）的提取和净化过程操作烦琐、回收率低。通过对净化条件进行优化,建立了加速溶剂萃取-在线净化-液相色谱串联质谱法检测污泥堆肥样品中TCS和TCC的分析方法,并对上海某污水厂实际污泥堆肥样品中的TCS和TCC进行定量分析。结果表明,TCS和TCC的检出限分别为0.003和0.0002μg/g,加标回收率为90.3%~99.8%,相对标准偏差（RSD）为1.2%~8.5%（n=6）。该方法样品前处理时间短、回收率高、试剂使用量少,能够满足实际污泥堆肥样品中TCS和TCC的检测要求。     

可燃气体燃爆特性综合试验装置构建与甲烷试验

为研究半开敞空间内可燃气体爆炸过程,设计带有泄压面的气体爆炸室,并在此基础上构建一套可燃气体燃爆特性综合试验装置。运用该试验装置,研究预混塔内甲烷气体分层现象以及甲烷爆炸浓度与最小点火能之间的变化规律。甲烷分层试验结果表明:静置一段时间后,预混塔中甲烷浓度随高度的增加而增大。最小点火能试验结果显示,当甲烷的试验爆炸体积分数在10%～13%时,其浓度与点火能之间呈现比较平缓的变化关系,而当其体积分数小于10%或大于13%时,浓度稍微变化,其点火能将发生明显变化。     

基于单片机甲烷浓度监测的研究

设计了一种基于单片机来实现的甲烷浓度检测和报警功能的系统,该检测系统以AT89S52单片机为核心,包括有电源电路、传感器采集电路、信号放大电路、红外遥控电路、声光报警电路、显示电路等功能模块组成,通过传感器采集电路采集信号,输出与甲烷浓度对应电压信号,把电压信号进行A/D转换后送入单片机,经单片机处理后驱动器显示出被测气体甲烷浓度值,若被测甲烷浓度大于报警电路预设数值,报警电路发出报警,可以及时切断供电系统,防止瓦斯爆炸事故的发生.该系统采用高精度敏感元件,集成运算放大器INA128,ADc0809,以及远距离高可靠性通信芯片,且具有高速的处理能力,是一种电路设计新颖,参数测量准确,操作方便的甲烷浓度报警监控系统,实现了数字瓦斯气体的实时监控.为实现数字化井下测控和可视化综合管理提供了切实可行的方案.     

油漆挥发分爆炸特性及浓度检测装置设计研究

为了实现对喷涂车间内挥发分浓度的检测，进行20 L球形爆炸特性测试实验，分析了油漆挥发分主成分及爆炸特性，根据油漆挥发分受热易挥发遇冷易凝结的物理特性、采样器采样原理、滤膜增重法测量原理以及基于单机片C++软件程序编写的电路智能控制技术，设计1种喷涂车间挥发分浓度检测装置。研究结果表明:油漆挥发分主成分具有爆炸性，且随着油漆颗粒物浓度增大，爆炸压力也增加。设计的装置对挥发分的采集率都在90%以上，总采集率为93.1%~98.9%，装置能够较为准确地检测挥发分浓度。     

Validation of a booted finite element model of the WIAMan ATD lower limb in component and whole-body vertical loading impacts with an assessment of the boot influence model on response

Objective: A novel anthropomorphic test device (ATD) representative of the 50th percentile male soldier is being developed to predict injuries to a vehicle occupant during an underbody blast (UBB). The main objective of this study was to develop and validate a finite element (FE) model of the ATD lower limb outfitted with a military combat boot and to insert the validated lower limb into a model of the full ATD and simulate vertical loading experiments.

Methods: A Belleville desert combat boot model was assigned contacts and material properties based on previous experiments. The boot model was fit to a previously developed model of the barefoot ATD. Validation was performed through 6 matched pair component tests conducted on the Vertically Accelerated Loads Transfer System (VALTS). The load transfer capabilities of the FE model were assessed along with the force-mitigating properties of the boot. The booted lower limb subassembly was then incorporated into a whole-body model of the ATD. Two whole-body VALTS experiments were simulated to evaluate lower limb performance in the whole body.

Results: The lower limb model accurately predicted axial loads measured at heel, tibia, and knee load cells during matched pair component tests. Forces in booted simulations were compared to unbooted simulations and an amount of mitigation similar to that of experiments was observed. In a whole-body loading environment, the model kinematics match those recorded in experiments. The shape and magnitude of experimental force–time curves were accurately predicted by the model. Correlation between the experiments and simulations was backed up by high objective rating scores for all experiments.

Conclusion: The booted lower limb model is accurate in its ability to articulate and transfer loads similar to the physical dummy in simulated underbody loading experiments. The performance of the model leads to the recommendation to use it appropriately as an alternative to costly ATD experiments.     

井下采空区构筑物漏风实测装置研发及应用

为了实时动态监测采空区构筑物漏风情况，自主研发了一种井下采空区构筑物漏风实测装置。通过现场实测及应用，研究结果表明:风流从工作面上进风口漏入采空区，而采空区中风流一部分通过与工作面之间的漏风流进入工作面下进风口，在下隅角位置附近形成一个涡流区；另一部分风流穿过沿空留巷构筑物进入留巷内，由于采空区的压实程度不同，采空区侧留巷内漏风速度曲线近似呈“L”型下降；通过收集分析留巷内漏风气体，其结果可反映采空区中瓦斯浓度分布情况，为采空区瓦斯治理提供了一种新的监测技术手段，且能有效地降低采空区瓦斯事故发生率，保证矿井的安全生产。