可调节常压边力拉深模设计

提出了以弹簧或橡胶作为弹性元件压边,可提供常压边力的新结构.采用这种压边方式,不仅可使压边力在拉深过程中保持不变,并能从零至最大设计压边力的范围内进行调节,且适用于不同厚度板坯的压边,故压边装置又具较大的通用性.     

玻璃纤维滤筒采集铅尘、铅烟预处理方法

探讨了一种快捷有效的降低玻璃纤维滤筒铅空白方法,即直接烘烤滤筒。该法操作简便,减少了试剂消耗量与操作时间。     

海洋环境监测中有关分析空白值的探讨

作者根据对《海洋监测规范》论证过程中提供的有关数据的统计分析,提出了样品检出限应高于样品空白的２倍,测定限应高于样品空白的３倍。亦即,一般情况下样品的测定限应高于空白值的３倍,若样品的测定值低于空白值３倍时,测定值将不可靠。     

30CrMnSiNi2A钢壳体毛坯的温挤压成形工艺研究

针对30CrMnSiNi2A超高强度钢制壳体毛坯的结构特点和材料工艺特性,对该壳体毛坯的温挤压成形工艺进行了大量的试验研究;并采用"正交试验方法"对温挤压工艺参数进行了优化设计。经过理化检测和使用结果表明,采用温挤压工艺生产的30CrMnSiNi2A钢制壳体毛坯锻件完全满足壳体的使用要求,各项性能指标合格。     

椭圆盒形拉延件合理毛坯的研究

利用保角变换由圆筒件拉延凸缘区的对数螺线推出椭圆盒形拉延件的滑移线方程 ,理论证明所求场满足边界条件和正交特性 ,并且与数值积分法的计算结果相当接近 ,最后给出了椭圆盒形拉延件合理毛坯的确定方法     

拼焊板材冲压成形技术(Ⅱ)

详细介绍和总结了拼焊板冲压成形的国内外研究与应用现状 ,讨论了拼焊板成形性能实验方法、拼焊板的不均匀变形规律、控制不均匀变形的方法以及计算机模拟方面的成果     

拼焊板在盒形件拉伸过程中的焊缝移动研究

分析了激光拼焊板在冲压成形过程中焊缝移动的基本原理 ,推导了单向拉伸情况下焊缝移动的基本公式 ;概述了拼焊板数值模拟建模的基本方法 ,并运用商业有限元软件AutoForm对盒形件拉伸过程中的焊缝移动进行了预测 ,将分析结果与国外实验结果进行对比 ,得出初始焊缝位置对焊缝移动的影响的基本规律     

氨氮测定时应注意的几个问题

纳氏试剂比色法是测定水中氨氮的国家标准方法[1].标准方法对氨氮的介绍比较详细,测定步骤也较简单,但实际工作中,情况比较复杂,条件较苛刻,实验空白值难以达到要求(A≤0.030),很多具体的因素都干扰影响该方法的灵敏度,也直接影响分析结果的精密度和准确度.根据多年的实际工作经验,将氨氮测定过程中容易出现的问题及注意事项进行了总结.     

Sources of polychlorinated biphenyl blank contamination and their impact on fingerprinting

Abstract

The development of high-resolution mass spectrometry methods for the measurement of polychlorinated biphenyls (PCBs) in environmental samples has dramatically reduced detection limits, leading to problems obtaining clean blanks. When PCBs are detected in samples at concentrations similar to the blanks, blank contamination must be addressed before fingerprinting and source apportionment through positive matrix factorization (PMF) can be successful. We tested a variety of blank correction methods using data from a study of water column concentrations of PCBs in the Spokane River, where concentrations of Σ₂₀₉PCBs in whole water samples averaged 171?pg/L without blank correction and Σ₂₀₉PCBs in the blanks averaged 88?pg/L. The results suggest that subtracting blank masses from sample masses can lead to erroneous results. Instead, censoring at one times the batch-specific blank level is a better approach. The sources of PCBs in field and method blanks were investigated by examining their congener profiles via PMF. The results suggest that commercial PCB formulations (in the US, Aroclors) continue to be the primary source of PCBs in blanks forty years after PCB production and use were banned in the United States. Other sources of PCBs to blanks include PCB 11 from pigments; PCBs 44?+?47?+?65, 45?+?51, and 68 arising from polymers cured using bis(2,4-dichlorobenzoyl) peroxide; and PCBs 1, 2, 3, 4, 8, 15 and others arising from silicone products derived from phenylsiloxanes, such as silicone-based adhesives.     

大气二氧化硫质控图的探讨

通过对全程序空白与已知浓度二氧化硫标准溶液的对照分析，提出了大气二氧化硫分析中质控图的做法。